Objective: The objective of this experiment is to use acid-base extraction techniques to separate a mixture of organic compounds based on acidity and/or basicity. After the three compounds are separated we will recover them into their salt forms and then purify them by recrystallization and identify them by their melting points. Procedure: Extraction of Carboxylic Acid A pre-weighed (0.315g) mixture of Carboxylic acid‚ a phenol‚ and neutral substance was placed into a reaction tube (tube 1)
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test for amino acids) Xanthoproteic Test Conc. HNO3‚ conc. NaOH For W‚F‚Y (aromatic except for H) Blue to blue-violet Oxidative decarboxylation color & deamination followed by (proline:hydroxypr condensation oline gives a yellow color) Yellow sol’n/ppt. Nitration via SEAr with conc. HNO3‚ orange with excess NaOH Millon’s rgt.(Hg2+ & Hg22+nitrates& nitriles/Hg(NO3)2 in conc. HNO3‚ w/ trace of HNO2/HgSO4‚H2SO4 ‚NaNO2) Hopkins-Cole Test Glyoxylic acid (Mg powder‚ oxalic
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Equilibrium and Acid Base Test Review: May 2012 Things to know: 1. Explain DYNAMIC EQUILIBRIUM. Why does a reaction at equilibrium look like it is NOT reacting? 2. Are all reactions equilibrium reactions? What assumptions do we make when we say that a reaction does NOT take place or that it is UNIDIRECTIONAL and goes 100% to completion 3. Be able to sketch a graph of the following (assuming that you start with all reactants and no products) : a. A reaction that really doesn’t do anything
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By: Jayquan S Salmond Out of all the amino acids‚ 8 are classified as essential amino acids. The body finds it hard to combine them with other compounds at a normal level to assist in adequate growth. The 8 are known as phenylalanine‚ valine‚ threonine‚ tryptophan‚ isoleucine‚ methionine‚ leucine‚ and lysine. When the isoleucine‚ leucine‚ and valine are grouped they are called BCAA or branched-chain amino acids. 1/3 of the body’s skeletal muscles are made up of BCAA. Skeletal muscles are
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Percent Acetic Acid in Vinegar Introduction: Acetic acid is reactive when combined with calcium carbonate. In this lab‚ we will use vinegar for its acetic acid and egg shells for their calcium carbonate. Marketable vinegar differs in its acetic acid concentration from 4-6%. Calcium carbonate reacts with the acetic acid in vinegar to produce carbon dioxide‚ water‚ and calcium acetate as represented by the equation: CaCO3 + 2HC2H3O2 CO2 + H2O + Ca(C2H3O2)2. The calcium carbonate reacts with
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Experiment 2: Centrifugation Title Centrifugation of fresh milk and Acetic Acid Objective(s): 1. To separate coagulated milk from mixture of fresh milk and Acetic Acid by centrifugation 2. To determine the relationship of speed of centrifugation with the coagulation of milk which separate from mixture. 3. To study the process of centrifugation Introduction Centrifugation is a process which materials suspended in a liquid medium undergo separation or concentrate due to the effect of gravity
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Interactive Physiology Worksheet: Fluid‚ Electrolyte‚ and Acid-Base Balance: Acid-Base Homeostasis 1. List the three important buffer systems in the body: protein buffer systems 1. _______________________________________________________________________ carbonic acid- bicarbonate system 2. _______________________________________________________________________ phosphate buffer system 3. _______________________________________________________________________ 2. Write the equation showing the relationship
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EXPERIMENT 4: Synthesis of Salicylic Acid from Wintergreen Oil Abstract: The purpose of this experiment is to take methyl salicylate (wintergreen oil) and by heating it under reflux with NaOH as a solvent‚ and then cooling the mixture with H2SO4 as another solvent‚ synthesize salicylic acid. The final step involves purify the product to produce as pure a sample of salicylic acid as possible. This process allowed for the successful production of 1.406g salicylic acid‚ an 82.70% yield. The NMR and IR
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Synthesis and Purification of Acetylsalicylic Acid (ASA or Aspirin) Background Salicylic acid is a phenol as well as a carboxylic acid. It can therefore undergo two different types of esterification reactions‚ creating an ester either with the hydroxyl or with the acid. In the presence of acetic anhydride‚ acetylsalicylic acid (aspirin or ASA) is formed. Correspondingly‚ an excess of methanol will form methyl salicylate‚ which is also an analgesic. In this experiment‚ we shall use
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BUTENEDIOIC ACID PRE-LAB ASSIGNMENT 1. Maleic acid is the cis version and fumaric acis is the trans version of butenedioic acid. 2. 3. See attached paper. 4. Maleic anhydride is the compound that crystalizes in part A in the experiment. 5. HCl acts as a catalyst to break one of the carbonyl group in the maleic acid which rotates the structure to form a trans structure of the butonal acid which is the fumaric acid. And it does so by donating its protons. 6. Maleic acid Chronic
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