October 9‚ 2013 Partner(s): Acetylsalicylic Acid Synthesis Theory. This experiment was carried out to see how the hydroxyl group on the benzene ring in salicylic acid reacts with acetic anhydride to form an ester‚ and to make aspirin. Synthesis of Acetylsalicylic Acid occurs by protonation of carbonyl (C=O) group‚ and a nucleophilic attack of OH on the acetic anhydride. The ferric chloride test and melting point were used to test the purity of the results. A hypothesized recovery rater of above
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also known as acetylsalicylic acid. C9H8O4 is the chemical format for Asprin. The chemical structure of aspirin: Aspirin is anti-inflammatory. Aspirin is prepared by chemical synthesis from salicylic acid‚ by acetylation with acetic anhydride. The fact that it is an acid allows us to quantify the amount of aspirin in a solution. We would do this by by using an acid-base titration. Sodium hydroxide (NaOH) will be used In this experiment as the base. Preparation • Lab coats should be fully fastened
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Citric acid cycle From Wikipedia‚ the free encyclopedia Jump to: navigation‚ search [pic] [pic] Overview of the citric acid cycle The citric acid cycle — also known as the tricarboxylic acid cycle (TCA cycle)‚ the Krebs cycle‚ or the Szent-Györgyi-Krebs cycle‚ [1][2] — is a series of enzyme-catalysed chemical reactions‚ which is of central importance in all living cells that use oxygen as part of cellular respiration. In eukaryotic cells‚ the citric acid cycle occurs in the matrix of the mitochondrion
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Standard Reduction Potentials‚ Equilibrium Constants and Investigating a Lead-Acid Electrolytic Cell Purpose Experimental Methods All procedures were followed according to the lab manual (experiment 10 – Electrochemistry Laboratory). Data and Observations Part A: Grams of FeSO4 used: 0.759 Voltage during voltmeter and battery check: 9.23V Table 1. Electrochemical Cells Data Part B: Table 2. Lead-Acid Battery Results and Calculations In order to make 5ml of 1M FeSO4(aq)
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of Acetylsalicylic Acid Abstract Acetylsalicylic acid was prepared using salicylic acid and acetic anhydride. As a result‚ a white‚ powdery substance was formed (0.1931g‚ percent yield 91.30%) and was defined by melting point (124.5 – 134.5°C) and observation of color change with ferric chloride. Introduction Acetylsalicylic acid (aspirin) is one of the most popular analgesic drugs on the market today. It also acts as an antipyretic and anti-inflammatory drug. Salicylic acid itself was too acidic
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ACIDS AND BASES The reason that acid-base reactions are so important is that many of the things you come into contact with on a daily basis are either acids or bases. Most fruits are acids‚ as are carbonated beverages‚ tea‚ and battery acid. Common household bases include baking soda‚ ammonia‚ soap‚ and antacids. What are acids and bases? There are not one but three common definitions used to describe acids and bases: 1. Arrhenius acids and bases 2. Brønsted-Lowry acids and bases 3. Lewis acids
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Vol. 1 ACETIC ACID 115 ACETIC ACID 1. Introduction Acetic acid [64-19-7]‚ CH3COOH‚ is a corrosive organic acid having a sharp odor‚ burning taste‚ and pernicious blistering properties. It is found in ocean water‚ oilfield brines‚ rain‚ and at trace concentrations in many plant and animal liquids. It is central to all biological energy pathways. Fermentation of fruit and vegetable juices yields 2–12% acetic acid solutions‚ usually called vinegar (qv). Any sugar-containing sap or juice can
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Acetylsalicylic Acid Experiment 01/25/2013 CHM Lab- 2211 Sec 0016 Instructor: Jennifer Reed Introduction: Commonly used as Aspirin‚ acetylsalicylic acid is an analgesic (pain reliever)‚ which is one of the products of the esterification reaction between salicylic acid and acetic anhydride. This esterification occurs since the hydroxyl group from the salicylic acid reacts with acetic anhydride to form an ester. In this experiment‚ we will be able to recreate this acid catalyzed reaction
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Abstract By using acid-base titration‚ we determined the suitability of phenolphthalein and methyl red as acid base indicators. We found that the equivalence point of the titration of hydrochloric acid with sodium hydroxide was not within the ph range of phenolphthalein’s color range. The titration of acetic acid with sodium hydroxide resulted in an equivalence point out of the range of methyl red. And the titration of ammonia with hydrochloric acid had an equivalence point that was also out of
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Flowers and Acid Call them freaks‚ the underground‚ the counterculture‚ flower children‚ or just simply hippies‚ they are all loose labels for the youth culture of the 60’s that transformed life in the West as we knew it‚ introducing the spirit of freedom‚ of hope‚ of happiness‚ of change‚ and of revolution (Miles 9). The years that made up the 1960’s were some of the most exciting and turbulent years in American history. The post World War II baby boomers grew up. A president and
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