alcohol) and acetic acid. It is mostly found in oranges and other citrus products. Octyl acetate can be synthesized by a condensation reaction: C8H17OH + CH3COOH → C10H20O2 + H2O Uses Because of its fruity odor‚ octyl acetate is used as the basis for artificial flavors and in perfumery. It is also as a solvent for nitrocellulose‚ waxes‚ oils and some resins. Source: http://en.wikipedia.org/wiki/Octyl_acetate Acetic Acid Acetic acid /əˈsiːtɨk/ (systematically named ethanoic acid /ˌɛθəˈnoʊɨk/)
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UNIVERSITI TEKNOLOGI MARA FAKULTI KEJURUTERAAN KIMIA ENGINEERING CHEMISTRY LABORATORY (CHE 485) GROUP : GROUP 1 EXPERIMENT : 1 - DETERMINATION OF THE CONCENTRATION OF ACETIC ACID IN VINEGAR DATE PERFORMED : 26TH OF SEPTEMBER 2013 SEMESTER : 1 PROGRAMME/CODE : EH220 - BACHELOR OF CHEMICAL ENGINEERING (HONS.) Table of content NO Title Allocated Marks (%) Marks 1 Abstract / Summary 5 2 Introduction 5 3 Aims 5 4 Theory 5 5 Apparatus 5 6
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(acetyl salicylic acid) from salicylic acid and acetic anhydride. CO2H OH salicylic acid 2g 0.014 mole O O O CH3 H2SO4 ethyl acetate CO2H O O acetyl salicylic acid acetic acid CH3 O + H3C + H3C OH acetic anhydride 5 mL 0.05 mole The limiting reagent is salicylic acid. The theoretical yield of acetyl salicylic acid is 2.52 g. Physical Data:* mp MW salicylic acid 157-9˚ 138 acetyl salicylic acid 135-6˚ 180 acetic anhydride — 102 acetic acid — 60 sulfuric acid — 98 ethyl acetate
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production (De Ory et al 2002). Acetic acid is the predominant flavoring and antimicrobial component in vinegar. Vinegar bacteria‚ also called acetic acid bacteria‚ are members of the genus Acetobacter and characterized by their ability to convert ethyl alcohol‚ C2H5OH‚ into acetic acid‚ CH3CO2H‚ by oxidation as shown below; Anaerobic Aerobic 2C2H5OH 2CH3CHO 2CH3CO2H + 2H2O Most bacteria strains derived from vinegar factories are able to oxidize acetic acid to CO2 and H2O (over-oxidation)
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Since a three-component system offers four degrees of freedom‚ temperature and pressure are held constant. A mixture of acetic acid‚ water and chloroform was studied in this experiment. A binodal curve was constructed by means of applying turbidimetric titration. Acetic acid-water mixture was titrated with chloroform and acetic acid-chloroform was titrated with water. The acetic acid composition was pre-assigned and the composition of each of the component in the mixture was determined and plotted in
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amount concentration of acetic acid in a sample of vinegar is 0.83 mol/L. VCH3COOH (aq) = 10.00 mL VNaOH (aq) = ? CCH3COOH = 0.83 mol/L CNaOH (aq) = 0.145 mol/L Materials: Sodium hydroxide 100 mL Acetic acid 50 mL 250 mL beaker x 2 Distilled water x 1 bottle Erlenmeyer flask x 1 Burette x 1 Pipette x 1 Pipette bulb x 1 Volumetric pipette x 1 Phenolphalein Procedure: Step 1- Gather materials‚ put on eyeglasses and apron. Step 2- Pour 50 mL of acetic acid into one 250 beaker
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Experiment 4 SOLUTION STOICHIOMETRY ACID-BASE TITRATIONS Determination of the Percent Acetic Acid in Vinegar Objectives: (1) To introduce and use the concept of solution stoichiometry (2) To specifically use solution stoichiometry to determine the percent of acetic acid in vinegar. (3) To prepare a standard solution by the method of titration. Consider the following balanced chemical equations: (1) HCl + NaOH ------> NaCl + HOH (2) H2SO4
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alcohol (1.0 mL) and excess glacial acetic acid(1.5 mL‚ 17.6M) were eppendorf pipetted into a 5 mL conical vile. This mixture was acid catalyzed by the addition on two drops of H2SO4. The mixture was then heated to 150-160⁰C in order to increase energy for esterification to occur over a period of 60- 75 minutes. The mixture then was cooled to room temperature before the addition of 5% aqueous sodium bicarbonate( 1.0 mL) in order to react excess acetic acid to form a the anionic form sodium acetate
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to test the product to see if it is within their acceptable ranges to be used. We will be synthesizing synthetic banana oil‚ or otherwise known as isopentyl acetate. We will synthesize thie oil by combining isopentyl alcohol with acetic acid and sulfuric acid‚ and heating under reflux for one hour. After this time‚ we will separate and purify our product via washing with sodium bicarbonate (that separates compounds via solubility properties) and distilling (that purifies via different boiling
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________________________ Internal Assessment Criteria Aspect 1 Aspect 2 Aspect 3 Total DCP CE Aim: The aim of this practical is to plot and investigate the pH titration curves for the titration of a strong acid with a strong base and of a weak acid with a strong base‚ and find Ka of the weak acid. Procedure: Part I 1. Pour 30 ml of the HCl solution of unknown concentration in a 100 ml beaker. 2. Add a stirring magnet. 3. Place the beaker on the magnetic heater and activate the rotating motor but not
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