Esterification and Hydrolysis: Methyl Benzoate by Fisher Esterification Nitration of Methyl Benzoate Jingling Li 2/16/2014 Purpose of the experiment: To understand the mechanisms for Fisher esterification reactions as an equilibrium process and hydrolysis is the reversal reaction of esterification. Nitrate methyl benzoate by an electrophilic aromatic substitution reaction. Summary of procedures: Add sulfuric acid to the mixture of benzoic and methanol‚ heat up the mixture to 65 oC
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Cyclohexene Synthesis by Dehydration Reaction of Cyclohexanol Gjulia Vokrri 02-15-2013 Abstract Alkenes can be produced by heating and dehydrating an alcohol in the presence of a strong acid. The purpose of this experiment was to synthesize cyclohexene by dehydration of cyclohexanol and to detect the presence of a double bond in the alkene. The dehydration reaction using distillation was
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The Grignard Synthesis of 3-methyl-3-heptanol In this experiment‚ an example of an organometallic compound which has a carbon magnesium bond will be utilized to form a tertiary alcohol. Grignard reagents have been extremely useful in the synthesis of a large number of classes of organic functional groups. Although Grignard reagents are unstable and decompose in air and moisture‚ they can be prepared and used immediately with moderate difficulty in the undergraduate organic chemistry laboratory
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That is‚ the entering group does not for the most part have the same position on the ring as that purged by the halogen substituent. Case in point‚ the hydrolysis of 4-chloromethylbenzene at 340° gives an equimolar mix of 3-and 4-methylbenzenols: Significantly all the more striking is the elite development of 3-methoxybenzenamine in the amination of 2-chloromethoxybenzene. Notice that this outcome is an infringement of the standard of minimum
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Question 2.1: (i) Calculate the number of electrons which will together weigh one gram. (ii) Calculate the mass and charge of one mole of electrons. * ------------------------------------------------- Answer (i) Mass of one electron = 9.10939 × 10–31 kg Number of electrons that weigh 9.10939 × 10–31 kg = 1 Number of electrons that will weigh 1 g = (1 × 10–3 kg) = 0.1098 × 10–3 + 31 = 0.1098 × 1028 = 1.098 × 1027 (ii) Mass of one electron = 9.10939 × 10–31 kg Mass of one mole of
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In order to first perform the reaction‚ 1.5 mL of 4-methylcyclohexanol was added to a pre-weighed 5mL conical vial. The conical vial was then weighed to find the actual mass of 4-methylcycloheaxanol. Then‚ 0.4mL of 85% phosphoric acid was added to the conical vial using a plastic pipet. Six drops of concentrated sulfuric acid was then added to the vial using a glass pipet. A spin vane was then added before adding the Hickman head‚ water condenser and a drying tube packed with calcium chloride to
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CHAPTER 4 Objectives: 1. Define consciousness.--------- 2. Appreciate the role of the circadian rhythm. 3. Describe the stages (5) of sleep including the sequence of the stages. The development of the electroencephalograph led to dramatic increases in what is known about sleep. When electrodes are attached to the face and scalp of sleepers‚ different patterns are produced on the graphic record called the electroencephalogram or EEG. The patterns vary in frequency and amplitude of the waves
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Pat 1 Synthesis of 4-aryl-6-indolylpyridine-2-carbonitriles and evaluation of their biological activity Synthesis of 6-indolyl-4-aryl-3-cyanopyridine-2-one (1a-e) Employing the MCRs approach and microwave irradiation‚ an equimolar amounts of aromatic aldehyde‚ 3-acetylindole‚ ethyl cyanoacetate were reacted with excess of ammonium acetate in one-pot‚ reaction‚ under the microwave irradiation‚ afforded a novel series of 4-aryl-6-indolyl-nicotinonitrile-2-one derivatives 1a-e. Ethylene glycol was
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passed Result: All hard drives (1) are using the NTFS file system. Detail: | Drive Letter | File System | | C: | NTFS | Issue: Password Expiration Score: Check failed (non-critical) Result: Some user accounts (2 of 4) have non-expiring passwords. Detail: | User | | Guest | | sec | Issue: Guest Account Score: Check passed Result: The Guest account is disabled on this computer. Issue: Autologon Score: Check passed
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13! (1 0.85)0 (0.85)130 (1 0.85)1 (0.85)131 0! (13 0)! 1! (13 1)! =0 . 1 2+ 0 09 . 2 7 7 =4 0.39= 839.83% Thus‚ the probability that the engineer incorrectly passes a day’s production as acceptable if only 85% of the day’s Blu-ray players actually conform to specification is 39.83%. (b) What is the probability that the engineer unnecessarily
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