Distillation Of Cyclohexane And Toluene

In the experiment of distillation we separated two miscible liquids. The purpose of distillation is to identify and purify compounds. We began our experiment by setting up an apparatus for macroscale simple distillation. We used 60 ml of Cyclohexane/ Toluene. We began with the temperature at 50 degrees Celsius. Unfortunately, we reached an error when the compounds evaporated too rapidly. The compounds evaporated so quickly that we lost data from 2 ml to 13 ml. The heat was lowered and as a result we started to see a constant rate. From 14 ml to 18 ml it stayed at the rate of 90 degrees Celsius, from 19ml to 25 ml it was at 93 from 26ml to 38ml it stayed in the 90’s for several minutes. When it reached the 50ml mark our temperature was at 108