| Preparation and standardization of 0.1 M NaOH using KHP | Analysis of unknown solid containing KHP | | Steanie Rodriguez | 6/7/2011 | CHEM-C311 Analytical Chemistry Laboratory July 7‚ 2011 The main purpose of this experiment is to identify an unknown organic acid by conducting various experiments to determine the acid’s unique properties. By determining selected constant properties of the unknown and then comparing these properties to the constant properties of known substances
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Formula: for NaoH N NaoH = grm KHP / ml NaoH x KHp /1000ml Formula: for HCL (NV) HCL = (NV) NaoH or N HCL V HCL = N NaOH V NaoH N HCL = VNAOH (NNaoH) / VHCL (for more info page 62-63 of the photocopy) KHP = Potassium hydrogen phthalate = KHC8H4O4 = Mw - 204.23 Trial 1: NNaoH = 1grm / 20.6 x 204.23 /1000 = 1grm / 4.21 = 0.24 normal NHCL = 20.6 (0.24) / 39.5 = 4.94 / 39.5 = 0.125 or 0.13 Trial 2: NNaoH = 1grm / 20.8 x 204.23 /1000
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Titration Lab of NaOH and KHP Aim: To titrate Sodium Hydroxide with Potassium Hydrogen Phthalate . To also determine the concentration of NaOH in the KHP solution. Hypothesis: When KHP is added to the solution of NaOH and the indicator‚ the solution will turn clear and neutralize. The concentration of NaOH is going to be very low because it is diluted. Materials required: pipette filler‚ volumetric flasks(2-4)‚ beakers(2)‚small white piece of paper‚ indicator( 2 drops)‚ conical flask‚ clamp
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SOLUTION PREPARATION AND STANDARDIZATION Submitted by Iris Olaso ______________________________________________________________________________ INTRODUCTION Generally‚ there are two ways in preparing a solution‚ one is by dissolving a weighed amount of solid in a required solvent and the other is by dilution of a concentrated solution into the desired concentration. In diluting concentrated solution‚ the concentration of the diluted solution can be determined by standardization. To standardize
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Preparation of the NaOH Solution Mass of NaOH before standing = NaOH before standing (g) – beaker (g) = 111.490 g – 110.970 g = 0.520 g Mass of NaOH after standing = NaOH after standing (g) – beaker (g) = 111.500 g – 110.970 g = 0.530 g Standardization of the NaOH solution TRIAL I Volume of NaOH solution = Final reading of buret - Initial reading of buret = 13.80 mL – 0.00 mL = 13.80 mL Converting the Volume (mL) to Volume (L) Volume (liters) = Volume (mL) x
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Experiment 5- Standardization of NaOH and determination of Molarity of an unknown Acid Objectives 1. Preparation and standardization of a 0.1M NaOH solution 2. To learn the technique of titration 3. Determination of the concentration of an unknown diprotic acid. Introduction Titration can be traced to the origins of volumetric analysis‚ which began in the late eighteenth century. Study of analytical chemistry began in France and the first burette was made by Francois Antoine Henri
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NaOH Standardization and Titration of an Unknown Organic Acid Overview: Methods for counting the number of molecules in a sample is a major emphasis of laboratory work. In this experiment we will use the method of titration to count the number of acid molecules in a solution. Measuring mass is a relatively easy procedure to do in the lab (although a balance is expensive). Counting the number of particles requires more effort. Molecular counting can be done by setting an unknown amount of a substance
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EXPERIMENT 10 Volumetric Analysis I Standardization of NaOH Solution Outcomes After completing this experiment‚ the student should be able to: 1. 2. 3. 4. Demonstrate the concept of quantitative analysis. Make solution and standardize it. Explain the difference between primary and secondary standard solutions. Quantitatively determine the concentration of a base. Introduction Titration is a common method of quantitative analysis used to determine the concentration of an unknown substance in a solution
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Title: Preparation and Standardization of a Sodium Hydroxide Solution Objective/Purpose: The objective of this experiment will be the standardization of sodium hydroxide using potassium hydrogen phthalate by the titration method. Introduction: The concentration of solutions can be reported in terms of molarity and normality. Molarity is equal to: HCL‚ HBR‚ H2SO4‚ HNO3 M = mol Solute (mol) (Monoprotic) (Diprotic) _______________ V(L)g solutions (L)
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ABABIO BUAHEN SAMUEL CHEMISTRY ONE REF. NO: 20216815 EXPERIMENT A.1.1.2 THE PREPARATION AND STANDARDIZATION OF NaOH AND HCL SOLUTION AIMS & OBJECTIVES: (1) To gain experience with titration procedure (2) To learn to standardize acid & base solution (3) To carry out the preparation of solution of a desired concentration (4) To carry out the preparation of solutions of desired concentration from more concentrated solution INTRODUCTION: Titration is a convenient quantitative method for accurately
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