In this experiment‚ the production of a Grignard reagent (phenylmagnesium bromide) was performed from a bromobenzene reactant combined with magnesium and ether. Phenylmagnesium bromide was then transformed into a tertiary alcohol called triphenylmethanol‚ through addition of another compound called benzophenone‚ as well as additional ether. The end product of triphenylmethanol was analyzed via NMR and IR. Figure 1: Preparation of the Grignard agent by combining bromobenzene with magnesium and ether
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Examples of synthesis reactions: 1. Metal + oxygen → metal oxide EX. 2Mg(s) + O2(g) → 2MgO(s) 2. Nonmetal + oxygen → nonmetallic oxide EX. C(s) + O2(g) → CO2(g) 3. Metal oxide + water → metallic hydroxide EX. MgO(s) + H2O(l) → Mg(OH)2(s) 4. Nonmetallic oxide + water → acid EX. CO2(g) + H2O(l) → ; H2CO3(aq) 5. Metal + nonmetal → salt EX. 2 Na(s) + Cl2(g) → 2NaCl(s) 6. A few nonmetals combine with each other. EX. 2P(s) + 3Cl2(g) →
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Cited: Aguilar‚ Andrea. "Synthesis of Aspirin Part B."CourseHero. N.p.. Web. 7 Mar 2014. . "aspirin." PubChem. National Center for Biotechnology Information. Web. 7 Mar 2014.
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system to isolate the alum. 2 Al(s) + 2 KOH + 22 H2O + 4 H2SO4 → 2 KAl(SO4)2●12H2O(s) + 3 H2(g) Its composition was analyzed using two precipitation tests and two flame tests. Three methods for growing crystals were then set up for observation next lab. Theoretical yield and percent yield: The theoretical yield for alum was 4.55g and the percent yield was 139%. The percent yield was above 100% because the alum was saturated with ethanol and water. KOH test: The KOH test identified the presence of
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Determining Allele Frequencies of the PV92 Alu Element using DNA Isolated from Human Cheek Cells and PCR Amplification Background Alu elements are the most abundant repetitive elements in the human genome that have mobilized throughout primate genomes by retrotransposition over the past 65 million years ago from a 5’ to 3’ fusion of the 7SL RNA gene‚ to reach the present number of more than one million copies. Over the last few years‚ several lines of evidence demonstrated that these elements
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Identify an unknown carbonyl compound © KCl http://hk.geocities.com/fatherofchemistry Objective To classify a carbonyl compound by a simple test and to identify it by the precipitation of a derivative. Principle In this experiment‚ the unknown compound is either an aldehyde or a ketone from Table 90. In the first part‚ on undergoing Tollen’s & Fehling’s tests‚ ketone will have no reaction. In the second part‚ by preparing a derivative of the compound with 2‚4-dinitrophenylhydrazine
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CHEM 1474-E01 Chemistry for Everyday WEEK5 Lab Report Spring 2017 Instructor: Kyoung Nan Kim Office: SI3076 Email: kyoung.kim@ucdenver.edu Office hour: M/W 1:00p-2:30p (SI3076) T/Th 12:30p-1:30p (SI3076) • All communication should be done via school email (xxxx@ucdenver.edu) • The work will be submitted through canvas assignments. You can simply upload doc/pdf files under “Lab report” assignment tap. • Review: Ch2‚ Ch3.5‚ Ch 4.2‚ Ch6.1 and Ch7.1-Ch 7.3 in your text book (21st
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Exp’t 84 Synthesis of Methyl Benzoate by Fisher Esterification from K. L. Williamson‚ Macroscale and Microscale Organic Experiments‚ 2nd Ed. 1994‚ Houghton Mifflin‚ Boston p385 Revised 10/15/03 Prelab Exercise: Give the detailed mechanism for the acid-catalyzed hydrolysis of methyl benzoate. Introduction: The ester group is an important functional group that can be synthesized in a number of different ways. The low-molecular-weight esters have very pleasant odors and indeed are the major components
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Thus a solution α-naphthol 1a‚ 4-methylbenzaldehyde 2a and tert-butyl isocyanide 3a in EtOH was magnetically stirred at 45 C for 12 hours under an oxygen atmosphere with an equimolar ratio of the three reactants. TLC monitoring of the reaction mixture exhibited formation of a new product‚ which was purified (Table 1‚ entry 1). Identification of its structure by NMR spectroscopy revealed that it was 2-(4-methylbenzoyl)-1-naphthyl N-(tert-butyl)carbamate (4a). Next‚ in order to improve the yield of
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In order to read DNA‚ it must be sequenced. This sequencing uses electrophoresis‚ a technique that separates sections of DNA that differ by a base. Electrophoresis used to be done manually‚ but was error prone and time consuming. Now‚ automatic sequencing machines are used. A technician begins the process by pouring gel between two glass plates that are set less than half a millimeter apart. After the gel is set up‚ DNA is put into each of the ninety-six lanes. The DNA sections then move through
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